Magnetic Force Microscopy
MFM
Magnetic properties imaging by sensing magnetic forces between a magnetized AFM tip oscillating above the sample surface
What is MFM (Magnetic Force Microscopy)
MFM measures magnetic domain structures by detecting variations in magnetic forces between a magnetized tip and sample surface, allowing visualization of nanoscale magnetic characterization.​
Unlike conventional AFM that measures surface topography through short-range forces, MFM detects long-range magnetic interactions between an AFM tip and the sample surface. A magnetically coated cantilever is oscillated near its resonant frequency while scanning the sample, and magnetic forces from the sample induce phase or frequency shifts, which are recorded as the MFM signal.
  • First pass acquires height signal in Non-contact mode
  • Second pass, the tip is lifted to a set (user-defined) height and follows the topography obtained from the first scan, allowing measurement of magnetic interactions without interference from surface features
Reasons to Use This Mode
Park Systems’ MFM offers two measurement modes to analyze magnetic domains with high flexibility and precision: ​Amplitude Modulation (AM)-MFM and Frequency Modulation (FM)-MFM.​

In AM-MFM, both the first height scan and the second lift scan use amplitude modulation. The magnetic force signal is detected as changes in oscillation amplitude or phase during the lift scan. This approach is straightforward and suitable for general magnetic contrast imaging. It is recommended to maintain a lift height greater than 30 nm to minimize crosstalk from surface features.​

​ In FM-MFM, while the first height scan still uses amplitude modulation to record topography, the second lift scan switches to frequency modulation to detect magnetic force gradients directly as frequency shifts. This results in improved sensitivity and higher spatial resolution. In this mode, a lower lift height (typically less than 10 nm) is recommended to enhance resolution and magnetic contrast.​
Applications and Use Cases
2205 stainless steel has a balanced microstructure of both austenite and ferrite phases. Unlike fully austenitic stainless steels, which are non-magnetic, it contains a significant amount of ferrite making it partially magnetic. MFM can be used to analyze 2205 stainless steel by mapping its magnetic domains, revealing variations in ferrite distribution and phase transformation effects.
  • Sample: 2205 Stainless Steel
  • System: NX10
  • Scan Size: 25 µm × 25 µm
GdFe is a ferrimagnetic alloy composed of gadolinium and iron, where Gd and Fe magnetic moments are aligned antiparallel, resulting in unique magnetic properties like high coercivity and tunable magnetization.​ MFM enables imaging of magnetic domains and mapping of the domain wall structure in GdFe by detecting phase or frequency shifts induced by magnetic forces from the sample.
  • Sample: GdFe
  • System: NX10
  • Scan Size: 5 µm × 5 µm
Option
Magnetic Field Generator (MFG)
MFM benefits significantly from the addition of a Magnetic Field Generator (MFG) module, which enables the application of controlled external magnetic fields to the sample under research. This capability allows detailed examination of magnetic domain behaviors, magnetization processes, and material property variations under diverse magnetic field orientations.
Park Systems' MFM offers an optional Field Switchable MFG module, providing maximum field intensities of ±6,000 G in-plane and ±2,000 G out-of-plane. By generating both in-plane and out-of-plane magnetic fields, the Field Switchable MFG expands the functionality of MFM, supporting comprehensive analyses of magnetic hysteresis, domain wall dynamics, coercivity, and anisotropy effects. In-plane fields are critical for observing phenomena such as domain wall motion and anisotropic magnetization, while out-of-plane fields are essential for exploring perpendicular magnetic anisotropy and spin reorientation. Together, these capabilities enable a comprehensive analysis of magnetic properties under versatile, three-dimensional field control with high spatial resolution.
Applications and Use Cases; Field Switchable MFG
MFM integrated with a Field Switchable MFG is crucial for in-situ characterization of magnetic materials. The changing domain structure of Pt/Co thin films on hBN flakes is clearly visualized by MFM phase images under increasing out-of-plane fields 60 G to 130 G, demonstrating the system's capability to study field-dependent magnetic behavior.
  • Sample: Pt/Co on hBN
  • System: NX10
  • Scan Size: 25 µm × 25 µm
MFM phase images capture the complex domain structure changes occurring in the permalloy sample as an in-plane magnetic field is applied. As the field increases from a low value of 10.9 G up to 46 G via intermediate steps like 35.1 G and 34.7 G, the rearrangement and deformation of the domain walls are clearly observed.
  • Sample: Permalloy
  • System: NX10
  • Scan Size: 28 µm × 43 µm
The MFM Phase images clearly demonstrate how the magnetic properties of the patterned structure change dramatically based on the direction of the applied 2,000 G field. By acquiring MFM phase images under zero field, 2,000 G in-plane, and 2,000 G out-of-plane field conditions, the results reveal how the external magnetic field direction and magnitude influence the magnetic domain configurations at the nanoscale, confirming the Field Switchable MFG's capability to control and study complex spin configurations in nanoscale devices.
  • Sample: Magnetic Material Patterned Wafer
  • System: NX10
  • Scan Size: 4 µm × 4 µm